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Beilstein J. Org. Chem. 2019, 15, 931–936, doi:10.3762/bjoc.15.89
Graphical Abstract
Scheme 1: The reaction of CSI with olefins.
Figure 1: The dipolar intermediate formed in the reaction of CSI with olefins.
Scheme 2: The synthesis of imide 9.
Scheme 3: The synthesis of ylidene sulfamoyl chloride 10.
Figure 2: (a) Molecular structure of racemic molecule 10 (asymmetric unit). Thermal ellipsoids are drawn at t...
Scheme 4: Mechanism for the formation of ylidenesulfamoyl chloride 10.
Figure 3: Relative energy profile of the reaction mechanism shown in Scheme 4.
Beilstein J. Org. Chem. 2011, 7, 1036–1045, doi:10.3762/bjoc.7.118
Scheme 1: Synthesis of anthracene oxides.
Scheme 2: Synthesis of methoxyanthracenes 10 and 11.
Figure 1: Molecular structure of compound 7. Displacement ellipsoids are shown at 40% probability level.
Scheme 3: The reaction mechanism for the formation of methoxyanthracenes 10 and 11.
Scheme 4: The formation mechanism for dihydroxy 17.
Figure 2: a) X-ray ORTEP plot of compound 17. Displacement ellipsoids are shown at 40% probability level. b) ...
Scheme 5: Base-promoted reaction of the dihydroxides and formation of the epoxides.
Scheme 6: Synthesis of compounds 27 and 28.